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Soc Am B 10, 587 (1993) 61 H J Eichler, R Menzel, B Sander, M Schulzke, and J Schwartz, SBS at different wavelengths between 308 and 725 nm, Opt Comm 121, 49 (1995) 62 D C Jones, Characterization of liquid Brillouin media at 532 nm, J Nonlinear Opt Phys Mater 6, 69 (1997) 63 H Yoshida, V Kmetik, H Fujita, M Nakatsuka, T Yamanaka, and K Yoshida, Heavy uorocarbon liquids for a phase-conjugated stimulated Brillouin mirror, Appl Opt 36, 3739 (1997) 64 M S Jo and C H Nam, Transient stimulated Brillouin scattering re ectivity in CS2 and SF6 under multipulse employment, Appl Opt 36, 1149 (1997)..

developed once a given physical parameter varies, which can then be speci cally modeled The spread of the NIR technique in the pharmaceutical industry was encouraged by advances in computer technology and data handling Both diffuse re ectance and transmittance measurements (Figure 10) are used, although diffuse re ectance much more widely because of its ease of use Many spectrometers were speci cally designed for the NIR range Instrument variety is wide and much more varied than in the MIR range The most sophisticated are dual-beam grating, diodearray, and FT instruments Simpler lter instruments are still available and remain valuable tools These instruments can basically be viewed as similar to those used for UV/Vis analysis Tungsten halogen lamps with quartz windows serve as sources Detectors are usually lead sul de (PbS) or arsine gallium (AsGa) detectors and many instruments are designed to operate from 180 to 2500 nm.

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The NIR spectra are less useful for identi cation and more useful for quantitative analysis of compounds containing functional groups made up of hydrogen bonded to carbon, nitrogen, or oxygen Such compounds can often be determined with an accuracy and precision equivalent to UV/Vis spectroscopy, rather than with MIR spectroscopy Many currently implemented applications concern the determination of water in variety of samples Re ectance NIRS has become a reliable tool for the quantitative determination of constituents in solids The rst use of this fast technique was for the determination of protein, moisture, starch, oil, lipids, and cellulose in feed and food products Sample handling, measurement procedure, and data treatment were established with these rst applications Typically in NIR the solid sample is irradiated with one or more narrow bands or the full range of radiation from 1 to 25 m.

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Diffuse re ectance occurs in which the radiation penetrates the surface layer of the particles, excites the vibrational modes of the analyte molecule, and is then scattered in all directions A re ectance spectrum is thus produced that is dependent upon the sample composition In this case the ordinate is the logarithm of the reciprocal of re ectance R, log(1/R), where R is the ratio of the intensity of radiation re ected from the sample to re ectance from a standard re ector, such as nely ground barium sulfate or magnesium oxide The typical re ectance band at 1940 nm is a water peak used for moisture determination, as can be seen in Figure 13 Many diffuse-re ectance instruments are available Some employ several interference lters to provide narrow bands of radiation Others are equipped with grating monochromators.

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